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Beilstein J. Org. Chem. 2014, 10, 3122–3126, doi:10.3762/bjoc.10.329
Graphical Abstract
Figure 1: Structures of aspergillides.
Scheme 1: Retrosynthetic analysis for (−)-aspergillide C.
Scheme 2: Synthesis of 11. Reaction conditions: (a) n-BuLi, THF/HMPA (5:1), −78 °C to rt, 12 h, 95%; (b) Li, t...
Figure 2: Key NOESY correlations observed in compound 11.
Scheme 3: Synthesis of 4 and formal total synthesis of (−)-aspergillide C (3). Reaction conditions: (a) [Cp*(...